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Customization Laboratory Vacuum Glove Box with Purification System
Closed Loop Gas Circulation
Inert gas in a closed loop. The gas is circulated by the blower and purifier, H2O, O2 can be removed continuously.
Auto Purging
The replacement of the atmosphere inside the glove box can be achieved automatically by the purging valves.
Automatic Regeneration
H2O and O2 removal material can be regenerated. The regeneration process can be program controlled.
Automatic Pressure Control
The pressure in the glove box is controlled automatically by the Programmable Logic Controller (PLC). Working pressure can be set between +10mba and -10mba. If the pressure goes over+/- 12mbar, the system will be protected automatically.
Eco Mode
The vacuum pump will be activated automatically when necessary, and will turn off after a period of idle time. Blower frequency will be switched to 25Hz when moisture and oxygen level reaches to less than 1 ppm
Structure
Integrated structure (Purification System integrated under the box)
Power Supply
110 - 220V AC, 50/60Hz, Single-phase
Glove box Box
Box Material 304 Stainless Steel (Type 304), thickness 3mm
Tray
Standard Layout
Two layers in box.
Option/Add: tool boxes or other
Various tool boxes, can be placed according to user needs.
Front window
Tilt design operating window, removable safety toughened glass front window, 8mm thickness,Wear resistance, corrosion resistance, good light transmission, sealing ring using 3/8 inch thick OMEGA sealing ring.
Option Window Open
The front window can be designed to open instead of fix, in order to put in a variety of instruments (custom function).
Environment of Box inside
H2O <1 ppm (20°C/68 ℉, 1 atm)
Antechamber
Control way: manual
Option/add auto control way
It will automatically control the antechamber by time setting and the number of times for gas exhaust and filling.
Option/Add: heating mode
Max temperature:200℃/ 392℉
Working gas and regeneration gas
Working gas: 99.999% high pure N2, Ar, He and other inert gas
Gas purification system
Single pure column:
Option dual columns purification system
Why choose duel pure column? 1,The Pure column need to be regenerated after saturated by absorbing the oxygen and moisture. The regeneration time is 16hours. If there is no reserved column, it may stop working. (we recommend dual column purification system to factory or other unit which need glove box working Continuously); 2,The pure capacity of dual pure columns is two times as much as single column
Pressure control system
Box pressure can be auto controlled by PLC touch screen
Filter system
The ends of inlet and outlet both are provided with filter
Closed circulating fan
High speed frequency conversion fan, flow 0-100m3/h, microprocessor control, Stainless steel device for pressure testing.
Control system
SIEMENS colors touch screen (6 inches), PLC control system, Bilingual in Chinese and English can be switched
measurements
Moisture analyzer: US GE brand, 0~1000ppm touch screen display, precision 0.1ppm
Oxygen analyzer: US GE brand, 0~1000ppm touch screen display, precision 0.1ppm
Vacuum Pump
Britain Brand EDWARDS, pumping speed 8.4-12m3/h, Model RV12
Glove
Brand: US NORTH
illumination system
Equipped with Fluorescent lamp. Brand: PHILIPS
Solvent removal system
Efficient adsorption of activated carbon, can effectively remove trace organic solvents;
Spare KF40 standard joint
Special design to KF40 Joint, you can lead the water into the box
Can be connected to other devices (low temperature refrigerator, film coating machine, microscope, solvent purification system, low temperature cold trap, heating furnace, etc.)
low temperature refrigerator
microscope
Solvent Purification System
Coating machine
Inside connection(one door of Coating machine is inside of glove box)
Equipment size and room requirements
Overall size
1850mm(L) x 1000mm(W) x 1950mm(H)
Room size
2200mm(L) x 1500mm(W) x 2000mm(H)
Wooden Package size and weight
2185mm(L) x 1145mm(W) x 2300mm(H)
650 kg (1400 lbs)
Notice
When the gas is circulating, must ensure that the piping of the circulation system is clear and cannot be blocked (if the color of the filter is changed from white to black, the filter should be replaced timely).
Box Size(excluded antechamber and support)1220mm(L) x 750mm(W) x 900mm(H)
47.2 " x 29.5" x 35.4"
Box Support height: 900mm(35.43" )
O2 <1 ppm (20°C/68 ℉, 1 atm)
Design: two circular antechambers
Main chamber size: Φ360mm (Dia.)x 600mm(length)(location: right-side of box)
14.17 "(Dia.) x 23.62" (L)
Mini chamber size: Φ150 mm(Dia.) x 300mm(L)(location: right-side of box)
5.9 "(Dia.) x11.8" (L)
Vacuum degree:<=-0.1MPa(right side antechambers included main chamber and mini chamber, all of that are need vacuum and display. The vacuum pressure gauge brand is German WIKA.
Control accuracy:±2℃/±3.6℉
The main chamber and mini chamber are both can adding the heating function (compared with standard antechamber the size is a little different)
Control gas:99.999% high pure inert gas
Regeneration gas: mixing gas of working gas and H2,hydrogen(H2)Volume accounted for 5-10%
If the pure system only has moisture removal function, the regeneration gas is the same with working gas
German BASF Oxygen removal material, US UOP high moisture absorb material. The regeneration process of purification system is auto control and automatic moisture and oxygen removal function.
Gas purity can be sustained and keep long-term:H2O<1ppm, O2<1ppm.
(one in use and the other is reserve)
Control accuracy:±1Pa
Can also be manually controlled by foot switch
The filter precision is: 0.3 mu m
With water cooling device (can equipped with water cooler and external refrigeration equipment)
Pressure sensor: -2500~2500Pa touch screen, accuracy±1Pa
Pressure control: control the box pressure to one setting point (scope can be set)
Extreme pressure 2 x 10-3 mbar/1.5 x 10-3 Torr
Inlet flange NW25
Outlet flange NW25
Noise level: 50 Hz 48 dBA
Material: Butyl
Model for standard 8B1532
Outside connection
72.83" x39.37" x 76.77"
86.6" x59" x 78.74"
86" x 45" x 91" (5.8M3)
No corrosive gas in the glove box.
It needs to regenerate the column when the moisture and oxygen indicators cannot meet the work requirements. If the corrosive gas is released from inside of glove box.(such as LiPF6 electrolyte),please do not use. you must put the bottle filled with liquid seal.
Vacuum pump needs to be checked the oil level and maintain in regular time.